<img src="https://secure.leadforensics.com/124134.png" style="display:none;">

About Scientificgear

By Hank Levi on Fri, Aug 31, 2012 @ 10:20 AM

describe the image

Scientificgear LLC provides several targeted areas of service including:

  • Karl Fischer Moisture Titration
  • Titration
  • Surface Tension (Tensiometers and Du Nouy Rings)
  • Contact Angle Analyzers for surface analysis
  • Thermal instruments (WBGT, Conductivity, Heat Flow)
  • Liquid Density Instruments (Benchtop and handheld)
  • Refractometers, Brix Meters

We support companies and organizations in select industries by providing:

  • Technical Support
  • Sales of Instruments
  • In-house and field repair service on select instruments
  • Calibration Service
  • Training and Installation
  • Some in-house testing
  • Manufacture and repair of Du Nouy Rings

Continue Reading

Karl Fischer Titration and Water Standard Presentation

By Hank Levi on Tue, Jun 28, 2011 @ 10:43 AM

Kf waterstandard presentation resized 600In this presentation we discuss the basic Karl Fischer Water Standards and talk about some of their uses for both Coulometric and Volumetric Karl Fischer Titration.  We also describe some of the related problems that can be identified and overcome by using Karl Fischer Water Standards.

Learn more about Karl Fischer Titration

Find more Coulometric Karl Fischer Titrator information

Learn more about Volumetric Karl Fischer Titration

 

Created on 06/28/11 at 10:48:28
Continue Reading

Calibrating Karl Fisher Titrators using water standards

By Hank Levi on Fri, May 20, 2011 @ 02:33 PM

“Calibrating” a Karl Fischer titrator is somewhat of a misnomer.MKC520 Karl Fisher Titrator What most operators are attempting to do is determine whether their Karl Fisher titrator is measuring moisture accurately.

A simple method is to run a water standard through the Karl Fischer Titrator like a normal direct injection test. Depending on the water standard you use, the result should equal a pre-determined level of moisture plus or minus a margin for error. These water standards are certified by the manufacturer (a certificate is included) to equal a precise level of moisture.

Learn more about the Karl Fischer 710 Series

We use Hydranal water standards. There are two kinds we typically use for coulometric Karl Fischer Titrators.

1) 0.1 normal

2) 1.0 normal.

The 0.1 normal administered at about 1mL should result in 100ppm (Parts Per Million) of moisture when measured. The acceptable result for this standard for the Karl Fischer titrator is +/- 10%. So your Karl Fischer Titrator should produce a reading between 90ppm and 110ppm to be in the acceptable range. If it is, you know your Karl Fischer Titrator is performing correctly.

Find more Coulometric Karl Fischer Titrator information

For the 1.0 normal everything is the same except the standard should result in 1,000ppm and your acceptable range is smaller at +/-3%. So your Karl Fischer Titrator should produce a reading between 970ppm and 1,030ppm.

Continue Reading

Recent Posts